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SONG Xinshu, CHEN Guoqing, ZHU Zhuowei, MA Chaoqun, ZHU Chun, ZHANG Xiaohe, LIU Huaibo, ZHU Conghai. Determination of volume fraction of acetic acid in Chinese aged liquor by 3-D fluorescence spectrometry[J]. LASER TECHNOLOGY, 2018, 42(4): 531-535. DOI: 10.7510/jgjs.issn.1001-3806.2018.04.018
Citation: SONG Xinshu, CHEN Guoqing, ZHU Zhuowei, MA Chaoqun, ZHU Chun, ZHANG Xiaohe, LIU Huaibo, ZHU Conghai. Determination of volume fraction of acetic acid in Chinese aged liquor by 3-D fluorescence spectrometry[J]. LASER TECHNOLOGY, 2018, 42(4): 531-535. DOI: 10.7510/jgjs.issn.1001-3806.2018.04.018
shu

Determination of volume fraction of acetic acid in Chinese aged liquor by 3-D fluorescence spectrometry

  • 1.

    School of Science, Jiangnan University, Wuxi 214122, China

  • 2.

    Jiangsu Provincial Research Center of Light Industrial Optoelectronic Engineering and Technology, Wuxi 214122, China

  • 3.

    School of Internet of Things Engineering, Jiangnan University, Wuxi 214122, China

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  • Received Date: June 25, 2017
  • Revised Date: October 16, 2017
  • Published Date: July 24, 2018
    Graphical Abstract
    • Abstract
  • In order to quickly determine the volume fraction of acetic acid in Chinese aged liquor, 3-D fluorescence spectroscopy and alternate fitting residual algorithm were used. Firstly, 3-D fluorescence spectra of different volume fraction of acetic acid of ethanol aqueous solution was used as the calibration set. 3-D fluorescence spectrum of liquor was used as the predicted set. Alternate fitting residual algorithm was used to analyze. Standard addition method was used to verify the accuracy of the results. Through theoretical analysis and experimental verification, the results show that, correlation coefficient between the predicted volume fraction and the experimental volume fraction is 0.9926. Average recovery percentage is 101.97%. 3-D fluorescence spectrometry combined with alternate fitting residual algorithm can quickly and effectively determine the volume fraction of acetic acid in Chinese aged liquor. This result is helpful for the detection of monomer volume fraction in Chinese aged liquor.
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    • References (18)
  • [1]
    ZHU S, LU X, JI K, et al.Characterization of flavor compounds in Chinese liquor Moutai by comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry[J]. Analytica Chimica Acta, 2007, 597(2):340-348. DOI: 10.1016/j.aca.2007.07.007
    [2]
    ZHU W H, CHEN G Q, ZHU Zh W, et al. Year prediction of a mild aroma Chinese liquors based on fluorescence spectra and simulated annealing algorithm[J]. Measurement, 2017, 97(11):156-164. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=cdd510bcb28f456246ac8feb43bcea96
    [3]
    YANG J L, ZHU T, XU Y, et al. Study on ultraviolet fluorescence spectra of monomers of distilled spirits[J]. Spectroscopy and Spectral Analysis, 2009, 29(12):3339-3343(in Chinese). http://www.ncbi.nlm.nih.gov/pubmed/20210165
    [4]
    TANG R. The relations of capproate bacteria, pit mud and Luzhou-flavour liquor[J]. Liquor Making, 2005, 32(4):24-27(in Chinese). http://en.cnki.com.cn/Article_en/CJFDTOTAL-NJZZ200504010.htm
    [5]
    ZHU Zh W, QUE L Zh, CHEN G Q, et al.Year discrimination of mild aroma Chinese liquors using three-dimensional fluorescence spectroscopy combinedwith parallel factor and neural network[J]. Spectroscopy and Spectral Analysis, 2015, 35(9):2573-2577(in Chinese). http://europepmc.org/abstract/MED/26669170
    [6]
    ZHU M, FAN W, XU Y, et al.1, 1-Diethoxymethane and methanethiol as age markers in Chinese roasted-sesame-like aroma and flavour type liquor[J]. European Food Research and Technology, 2016, 242(11):1985-1992. DOI: 10.1007/s00217-016-2697-x
    [7]
    HAN S, ZHANG W, LI X, et al. Determination of three alcohols in Chinese Dukang base liquor by FT-NIR spectroscopy[J]. Food Analytical Methods, 2016, 9(8):2194-2199. DOI: 10.1007/s12161-016-0403-z
    [8]
    MA L, SHEN X M, LI A J, et al. Determination of the content of lactic acid & acetic acid by HPLC[J]. Sichuan Food and Fermentation, 2016, 52(1):84-86(in Chinese). http://d.old.wanfangdata.com.cn/Periodical/spgykj201716047
    [9]
    WU J F, XU Y.Comparison of pyrazine compounds in seven Chinese liquors using headspace solid-phase micro-extraction and GC-nitrogen phosphourusdetection[J]. Food Science and Biotechnology, 2013, 22(5):1-6. DOI: 10.1007/s10068-013-0209-3
    [10]
    ZHU W, REN C, NIE Y, et al.Quantification of ochratoxin a in Chinese liquors by a new solid-phase extraction clean-up combined with HPLC-FLD method[J]. Food Control, 2016, 64(6):37-44. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=f661f4e370bb47b26963ec988d25dc86
    [11]
    CHEN G Q, WU Y M, WANG J, et al. Fluorescence spectroscopy study of synthetic food colors[J]. Spectroscopy and Spectral Analysis, 2009, 29(9):2518-2522(in Chinese). http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=gpxygpfx200909050
    [12]
    ZHUNAG Y, MA Ch Q, WANG X H, et al. Simultaneous determination of three antibiotics based on synchronous fluorescence combined with neural network[J]. Laser Technology, 2017, 41(4):489-493(in Chinese). http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=jgjs201704006
    [13]
    DU J M, CHEN G Q, MA Ch Q, et al. Determination of carmine concentration with 3-D synchronous fluorescence spectrometry[J]. Laser Technology, 2017, 41(4):489-493(in Chinese). http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=jgjs201704009
    [14]
    URÍČKOVÁ V, SÁDECKÁ J, MÁJEK P.Classification of Slovak juniper-flavoured spirit drinks[J]. Journal of Food & Nutrition Research, 2015, 54(4):425-429. DOI: 10.1007/s12161-014-9869-8
    [15]
    ELCOROARISTIZABAL S, CALLEJÍN R M, AMIGO J M, et al.Fluorescence excitation-emission matrix spectroscopy as a tool for determining quality of sparkling wines[J]. Food Chemistry, 2016, 206(9):284-290. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=234ccdd7ad5ee7c42f8ce4b7a07c3bed
    [16]
    ZHONG X D, FU D S, WU P P, et al.Rapid fluorescence spectroscopic screening method for the sensitive detection of thiabendazole in red wine[J]. Analytical Methods, 2014, 6(18):7260-7267. DOI: 10.1039/C4AY00991F
    [17]
    WU H L, NIE J F, YU Y J, et al. Multi-way chemometric methodologies and applications:a central summary of our research work[J]. Analytica Chimica Acta, 2009, 650(1):131-142. DOI: 10.1016/j.aca.2009.05.041
    [18]
    XIA A L, WU H L, FANG D M, et al. A novel trilinear decomposition algorithm for second-order linear calibration[J]. Chemometric and Intelligent Laboratory Systems, 2000, 52(1):75-86. DOI: 10.1016/S0169-7439(00)00081-2
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