Abstract: In this paper,the adhesive strength between photopolymerizated film,glass substrate and CD's Ni-Stamper has been measured.We separately use three methods:pre-coating a thin layer of PMMA,SOL-GEL processing,dipping coating a thin layer of α-replaced silicane connective,to improving the adhesive quality of glass substrate' surface and then compare these methods through different facets to select the simplest and most economical technology.A copy of Ni-Stamper of CD is made by this technology,the microstructure of the copied information is given here with SEM.