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Volume 35 Issue 5
May  2013
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Raman spectrum analysis of forsythia leaves

  • Received Date: 2010-09-29
    Accepted Date: 2010-12-10
  • In order to assess the quality of the forsythia leaves gathered in different periods rapidly, their Raman spectra were obtained with RM-1000 confocal microscopy laser Raman spectrometer, then the specific peaks of their Raman spectra were obtained after analysis and experiments. The Raman spectra of forsythia leaves show the main characteristic peaks are mainly in the range of 700cm-11600cm-1 and 2600cm-13100cm-1. The characteristic peaks are closely related with forsythin which is considered as the main active ingredient in the forsythia leaves and can be used for qualitative identification. The peak intensity in the spectra of forsythia leaves gathered in different periods is significantly different so that the quality of forsythia leaves can be evaluated. Raman spectra can be used for qualitative identification and evaluation of forsythia Leaves and it is direct, fast, simple and accurate. The results are useful for quality control of the traditional Chinese medicine.
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  • [1]

    WU L,OUYANG Zh H,CAO Sh Ch,et al.Research development and application of Raman scattering technology[J].Chinese Journal of Light Scattering,2005,17(2):180-186(in Chinese).ZHANG Q M,ZHANG X,LIU Zh X.Study on identification of principal constituent of fever-relieved and pain-refieved drugs by the handheld Raman spectrometer[J].Chinese Pharmaceutical Journal,2008,43(24):1903-1906(in Chinese).
    [2]

    ZHANG Q M,ZHANG X,LIU ZH X.Study on identification of principal constituent of fever-relieved and pain-refieved drugs by the handheld Raman spectrometer[J].Chinese Pharmacenutical Joumal,2008,43(24):1903-1906(in Chinese).
    [3]

    QU X B,ZHAO Y,SONG Y,et al.Raman spectroscopy study on the structure of ginsenoside Rg3 [J].Spectroscopy and Spectral Analysis,2008,28(3):569-571(in Chinese).
    [4]

    LIU W H,YANG W,WU X Q,et al.Direct determination of ethanol by laser Raman spectra with internal standard method[J].Chinese Journal of Analytical Chemistry,2007,35(10):1503-1505(in Chinese).
    [5]

    XU L L,DING K K,GUO X Q,et al.Raman spectra of salicylic acid,p-methoxybenzoic acid and metronidazole[J].Journal of Capital University of Medical Sciences,2006,27(6):785-787(in Chinese).
    [6]

    ZHAO Y Zh,LI Z W,GAO Sh Q,et al.Ultra-trace analysis of biological molecules in water by means of the resonance Raman spectra in liquid-core optical fiber[J].Laser Technology,2004,28(5):491-493(in Chinese).
    [7]

    NAN N,SHAO Y H,JIANG Y L,et al.Study of carotenoid in human skin by means of resonance Raman detection[J].Laser Techno-logy,2008,32(5):490-492(in Chinese).
    [8]

    YANG Ch H,SHI X H,LIU X B,et al.Study of Raman spectrum in detecting mineral substance concentration of drinking water[J].Laser Technology,2008,32(4):366-369(in Chinese).
    [9]

    WU X Q,ZHENG J Zh,LIU W H,et al.Quantitative determination of glucose by internal standard laser Raman spectra[J].Spectroscopy and Spectral Analysis,2007,27(7):1344-1346(in Chinese).
    [10]

    BELU A,MAHONEY C,WARMOUTH K.Chemical imaging of drug eluting coatings:combining surface analysis and confocal Raman microscopy[J].Journal of Controlled Release,2008,126(2):111-121.
    [11]

    ZHANG L,HENSON M,SEKULIC S.Multivariate data analysis for Raman imaging of a model pharmaceutical tablet[J].Analytica Chimica Acta,2005,545(2):262-278.
    [12]

    ZHANG G,LI F R,DUAN F,et al.Determination of phillyrin,forsythiaside and rutin in folium forsythia gathered in different periods[J].Natural Product Research and Development,2005,17(6):790-793(in Chinese).
    [13]

    LI F R,DUAN F,YANG J X.Comparative study on content of phillyrin in fructus forsythiae and leaves of forsythia (forsythia suspensa)[J].Acta Botanica Boreali-Occidentalia Sinica,2004,24(4):725-727(in Chinese).
    [14]

    ZHU S Y,YANG J X,LI F R.Effects of forsythia suspense leaves' extract on oxidative lesion in mice[J].Pharmacology and Clinics of Chinese Materia Medica,2004,20(1):18-20(in Chinese).
    [15]

    WU Y F,WANG X Sh,SHANG X J.Determination of phillyrin in green and grown fructus forsythiae from funiushan[J].Lishizhen Medicine and Materia Medica Research,2008,19(4):855-856(in Chinese).
    [16]

    ZHU Z Y,GU R A,LU T H.Raman spectroscopy in chemistry[M].Shengyang:Northeastern University Press,1998:79-84(in Chinese).
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    沈阳化工大学材料科学与工程学院 沈阳 110142

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Raman spectrum analysis of forsythia leaves

  • 1. College of Pharmacy, Henan University, Kaifeng 475004, China;
  • 2. College of Physics and Electronic Information, Henan University, Kaifeng 475004, China

Abstract: In order to assess the quality of the forsythia leaves gathered in different periods rapidly, their Raman spectra were obtained with RM-1000 confocal microscopy laser Raman spectrometer, then the specific peaks of their Raman spectra were obtained after analysis and experiments. The Raman spectra of forsythia leaves show the main characteristic peaks are mainly in the range of 700cm-11600cm-1 and 2600cm-13100cm-1. The characteristic peaks are closely related with forsythin which is considered as the main active ingredient in the forsythia leaves and can be used for qualitative identification. The peak intensity in the spectra of forsythia leaves gathered in different periods is significantly different so that the quality of forsythia leaves can be evaluated. Raman spectra can be used for qualitative identification and evaluation of forsythia Leaves and it is direct, fast, simple and accurate. The results are useful for quality control of the traditional Chinese medicine.

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