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Volume 29 Issue 6
Sep.  2013
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Preparation of Fe73.5Cu1Nb3Si13.5B9 nanocrystalline bulk by laser-remelting

  • Received Date: 2004-10-26
    Accepted Date: 2005-01-18
  • After quickly remelting Fe73.5Cu1Nb3Si13.5B9 amorphous ribbons by laser,nanocrystalline bulk is gained when tiny melted pools solidified rapidly.The size of nanocrystalline bulk depends on the laser-remelting.When the input laser facula diameter is 20mm~40mm,the output facula diameter is about 2mm and!the scanning speed is 5mm/s,the nanocrystalline bulk can reach up to 2mm and the length and width are not limited.Analysis of its configuration indicates that the main phase in nanocrystalline bulk is α-Fe,the crystal constant of α-FeSi is about 25nm.At the same time,a lot of spherical Nb-rich areas appear.
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    [2] 张甫飞,张洛,纪朝廉 et al.纳米晶软磁合金材料及应用[J].上海金属,2002,24(1):21~26.

    [3] 宋翀旸,陈学定,俞伟元 et al.Fe基非晶软磁合金的纳米晶化及磁性[J].甘肃工业大学学报,2003,29(2):14~17.

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    DUHAJ P,SVEC P,SITED J et al.Thermodynamic,kinetic and structural aspects of the formation of nanocrystalline phase in Fe76Cu1Nb3Si13.5B9 alloy[J].Materials Science and Engineering,2000,A304~A306:178~186.
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    FRANCO V,CONDE C F,CONDE A et al.Surperparamagnetic behaviour in Fe-Cu-Nb-Si-B alloy[J].Journal of Magnetism and Magnetic Materials,2000,214~216:400~403.
    [6] 陈岁元,刘常升,才庆魁 et al.激光晶化制备Fe基纳米软磁材料的研究进展[J].激光技术,2005,29(1):94~97.

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    ZHANG J W,ZHANG X Y,XIAO F R et al.Influence of additive elements Nb and Mo on the crystallization process of amorphous alloy Fe76.5Cu1Si13.5B9[J].Mater Lett,1998,36:223~228.
    [8] 韦世强,李忠瑞,张新夷 et al.超细Ni-B 非晶态合金的退火晶化及其催化性能[J].科学通报,2000,45(18):1941~1943.

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    沈阳化工大学材料科学与工程学院 沈阳 110142

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Preparation of Fe73.5Cu1Nb3Si13.5B9 nanocrystalline bulk by laser-remelting

  • 1. School of Materials Science and Engineering, Nanchang University, Nanchang 330047, China

Abstract: After quickly remelting Fe73.5Cu1Nb3Si13.5B9 amorphous ribbons by laser,nanocrystalline bulk is gained when tiny melted pools solidified rapidly.The size of nanocrystalline bulk depends on the laser-remelting.When the input laser facula diameter is 20mm~40mm,the output facula diameter is about 2mm and!the scanning speed is 5mm/s,the nanocrystalline bulk can reach up to 2mm and the length and width are not limited.Analysis of its configuration indicates that the main phase in nanocrystalline bulk is α-Fe,the crystal constant of α-FeSi is about 25nm.At the same time,a lot of spherical Nb-rich areas appear.

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